ANALYSIS OF TOXICOLOGICAL CHEMISTRY II

Academic Year 2022/2023 - Teacher: RITA TURNATURI

Expected Learning Outcomes

Provide theoretical and practical tools to carrying out qualitative analyzes of toxic inorganic, organometallic and organic elements and compounds. The student acquires in the laboratory the skills necessary for the execution of manual and instrumental analyses.

Course Structure

Teaching methodology

The teaching is divided into lessons and laboratory experiences. PIT "tests in progress" are envisaged, in the form of short-themed questions or multiple-choice tests.

Required Prerequisites

Knowledge of General and Inorganic Chemistry, Organic Chemistry, Toxicological Chemistry

Attendance of Lessons

8 CFU of which:

5 CFU frontal lessons (35 hours in the classroom and ongoing tests PIT)
2 CFU group laboratory experiences (24 hours)
1 CFU individual laboratory experiences (15 hours)

Detailed Course Content

FIRST MODULE

WATER, SOIL, AIR pollution. Nature and classes of organic, inorganic and metallorganic pollutants of water, soil and air. Conventional and innovative methods for the treatment of water, soil and air. Water treatment for drinking, domestic and industrial use. Qualitative analysis of cations and anions: "dry and wet". APAT METHODS.

SECOND MODULE

Environmental Chemical Analysis Sampling. Water analysis. Atmospheric monitoring. Soil analysis. Instrumental methods of analysis: Classical methods. Methods classification.

Optical Methods: Theoretical principles and generalities on Flame Photometry, UV-Visible Spectroscopy and Atomic Absorption Spectroscopy, IR Spectroscopy, Mass Spectroscopy.

Chromatographic Methods: Theoretical principles, generalities and classification. Thin Layer Chromatography (TLC) and High Performance Liquid Cromatography (HPLC). Ion exchange chromatography (IEC).

Textbook Information

1) C. Baird, M. Cann. “Chimica Ambientale” Zanichelli.

2) Araneo.“Chimica analitica qualitativa”Casa Editrice

Ambrosiana.

3) Baue, Christian, O'Reilly.“Analisi Strumentale”Piccin-

4) C. Marzano, C. Medana “Chimica Tossicologica” Piccin.

5) S.E.Manahan.“Chimica dell’ambiente” Piccin.

Author	Title	Publisher	Year	ISBN
C. Baird, M. Cann	Chimica Ambientale	Zanichelli	2013	9788808173782
Araneo	Chimica analitica qualitativa	Casa Editrice Ambrosiana	1993	9788808080189
Baue, Christian, O'Reilly	Analisi Strumentale	Piccin	1985	8829903604
C. Marzano, C. Medana	Chimica Tossicologica	Piccin	2017	978-88-299-2875-0
S.E.Manahan	Chimica dell’ambiente	Piccin	2000	978-8829913879

Course Planning

	Subjects	Text References
1	WATER, SOIL, AIR pollution.	C. Baird, M. Cann. “Chimica Ambientale” ZanichelliC. Marzano, C. Medana “Chimica Tossicologica” Piccin.
2	Nature and classes of organic, inorganic and metallorganic pollutants of water, soil and air. Conventional and innovative methods for the treatment of water, soil and air.	C. Baird, M. Cann. “Chimica Ambientale” ZanichelliC. Marzano, C. Medana “Chimica Tossicologica” Piccin.C. Marzano, C. Medana “Chimica Tossicologica” Piccin.
3	Water treatment for drinking, domestic and industrial use. Qualitative analysis of cations and anions: "dry and wet". APAT METHODS.	C. Baird, M. Cann. “Chimica Ambientale” ZanichelliC. Marzano, C. Medana “Chimica Tossicologica” Piccin.
4	Qualitative analysis of cations and anions: "dry and wet".	Araneo.“Chimica analitica qualitativa”Casa Editrice Ambrosiana.
5	APAT METHODS	Material provided by the teacher
6	Environmental Chemical Analysis	S.E.Manahan.“Chimica dell’ambiente” Piccin. Material provided by the teacher.
7	Sampling: Water analysis. Atmospheric monitoring. Soil analysis. Instrumental methods of analysis: Classical methods. Methods classification.	S.E.Manahan.“Chimica dell’ambiente” PiccinC. Marzano, C. Medana “Chimica Tossicologica” Piccin.Material provided by the teacher.
8	Instrumental methods of analysis: classical methods.Methods classification.	Baue Christian, O'Reilly.“Analisi Strumentale”. Piccin.Material provided by the teacher.
9	Optical Methods: Theoretical principles and generalities on Flame Photometry, UV-Visible Spectroscopy and Atomic Absorption Spectroscopy, IR Spectroscopy, Mass Spectroscopy.	Baue Christian, O'Reilly.“Analisi Strumentale”. Piccin.Material provided by the teacher.
10	Chromatographic Methods: Theoretical principles, generalities and classification. Thin Layer Chromatography (TLC) and High Performance Liquid Cromatography (HPLC). Ion exchange chromatography (IEC).	Baue Christian, O'Reilly.“Analisi Strumentale”. Piccin.Material provided by the teacher.

Learning Assessment

Learning Assessment Procedures

Learning verification methods

The course is divided into lessons and single and group laboratory experiences. "Progressive tests" PIT are envisaged, in the form of short-themed questions or multiple-choice tests.

Exam

The exam consists of a written paper aimed to ascertain the knowledge of the topics proposed and the ability to represent the phenomena and chemical reactions of the toxicological analysis.

Information for students with disabilities and/or DSA.

To guarantee equal opportunities and interested students can request a personal interview in order to plan any compensatory and/or dispensatory measures, based on the educational objectives and specific needs. It is also possible to contact the CInAP (Centre for Active and Participatory Integration - Services for Disabilities and/or DSA) referent professor of our Department, Prof. Teresa Musumeci

Examples of frequently asked questions and / or exercises

1) Fourth group cations search and recognition .

2) Halides search and recognition.

3) Flame Test.

4) TLC.

5) UV-Vis spectroscopy.

Degree Course in

Applied Pharmaceutical Sciences